{"id":158,"date":"2021-05-20T05:43:38","date_gmt":"2021-05-20T05:43:38","guid":{"rendered":"http:\/\/localhost\/nuc\/?p=158"},"modified":"2025-03-11T13:05:13","modified_gmt":"2025-03-11T13:05:13","slug":"materiale-nucleare-si-coroziune","status":"publish","type":"post","link":"http:\/\/nuclear.ro\/en\/materiale-nucleare-si-coroziune\/","title":{"rendered":"Nuclear Materials, Corrosion and Surface Analysis"},"content":{"rendered":"<div data-elementor-type=\"wp-post\" data-elementor-id=\"158\" class=\"elementor elementor-158\" data-elementor-settings=\"[]\">\n\t\t\t\t\t\t\t<div class=\"elementor-section-wrap\">\n\t\t\t\t\t\t\t<section class=\"elementor-section elementor-top-section elementor-element elementor-element-1c4e2d33 elementor-section-boxed elementor-section-height-default elementor-section-height-default sc_fly_static\" data-id=\"1c4e2d33\" data-element_type=\"section\">\n\t\t\t\t\t\t<div class=\"elementor-container elementor-column-gap-extended\">\n\t\t\t\t\t<div class=\"elementor-column elementor-col-100 elementor-top-column elementor-element elementor-element-26d427cb sc_inner_width_none sc_content_align_inherit sc_layouts_column_icons_position_left sc_fly_static\" data-id=\"26d427cb\" data-element_type=\"column\">\n\t\t\t<div class=\"elementor-widget-wrap elementor-element-populated\">\n\t\t\t\t\t\t\t\t<div class=\"elementor-element elementor-element-2c83b315 animation_type_block sc_fly_static elementor-widget elementor-widget-text-editor\" data-id=\"2c83b315\" data-element_type=\"widget\" data-widget_type=\"text-editor.default\">\n\t\t\t\t<div class=\"elementor-widget-container\">\n\t\t\t\t\t\t\t<p><strong><u>Thermomechanical Properties and Microstructural Analyzes<\/u><\/strong><\/p><p><strong>Activities<\/strong><\/p><ul><li>Microstructural analysis by optical microscopy, scanning electron microscopy (SEM) and energy dispersive X-ray spectrometry of metallic and ceramic materials;<\/li><li>Teste termo-mecanice pe materiale metalice,\u00a0 ceramice \u0219i compozite \u00een intervalul de temperatur\u0103 20 \u00f7 1000<sup>o<\/sup>C (trac\u021biune, fluaj, ciclaj, mecanica ruperii);<\/li><li>Explosion tests on thin-walled tubes at room temperature;<\/li><li>Hydrogen and oxygen content analysis on samples of steel and alloys based on titanium and zirconium;<\/li><li>Hydration of samples from nuclear structural materials;<\/li><li>Uniaxial stress tests (SSRT traction and creep) in molten lead environment.<\/li><\/ul><p><strong>IAEA Vienna Cooperation and European Projects<\/strong><\/p><ul><li class=\" translation-block\">CRP 17519 \u2013 Prediction of Axial and Radial Creep in HWR Pressure Tubes;<\/li><li class=\" translation-block\">CRP 16705 \u2013 Benchmarking of advanced materials pre-selected for innovative nuclear reactors;<\/li><li class=\" translation-block\">FP7 MatISSE \u2013 GA 604862: Materials\u2019 Innovations for a Safe and Sustainable nuclear in Europe;<\/li><li class=\" translation-block\">GEMMA (GEneration iv Materials Maturity), GA 755269, in the framework of EERA AISBL (JPNM \u2013 SP1 ESNII and SP2 Inovative steels);<\/li><li class=\" translation-block\">PATRICIA (Partitioning And Transmuter Research Initiative in a Collaborative Innovation Action), GA 945077.<\/li><\/ul><p><strong>Main achievements<\/strong><\/p><ul><li>Expertise in failure analysis and diagnosis of degraded components from Cernavoda NPP;<\/li><li>Development of experimental devices for tensile tests in molten lead;<\/li><li>Tensile tests on generation IV structural materials, in molten lead medium;<\/li><li>Scientific activities in international projects: MATISSE, IAEA CRP, GEMMA.<\/li><\/ul><p><strong><u>Corrosion<\/u><\/strong><\/p><p><strong>Activities<\/strong><\/p><ul><li>Corrosion tests at high temperatures and pressures in static and dynamic regime, in operating conditions specific to the CANDU reactor;<\/li><li>Investigation of the mechanisms of release, transport and deposition of corrosion products in the heat transfer circuits of the CANDU plant;<\/li><li>Analysis of corroded components in nuclear installations, identification of causes and establishment of measures to reduce \/ prevent corrosion phenomena;<\/li><li>Studies on microbiological corrosion in nuclear installations;<\/li><li>Development of procedures in accordance with national and international standards for the application of new methods of analysis;<\/li><li>Teste de coroziune\u00a0 \u00een mediu de plumb lichid;<\/li><li>Corrosion tests in water environment at supercritical temperatures;<\/li><li>Participare \u00een proiecte interna\u021bionale, \u00een domeniul test\u0103rii la coroziune a materialelor structurale pentru reactori nucleari de GEN III \u0219i IV (proiecte H2020 \u2013 MEACTOS, ECC-SMART).<\/li><\/ul><p><strong>Main achievements<\/strong><\/p><ul><li class=\" translation-block\">Dynamic on-load cracking corrosion testing of samples from Inconel 182 and 316L steel at high temperatures and pressures (2880C, 90bar, 2ppm O dissolved) with different traction speeds within the MEACTOS H2020 project;<\/li><li>Identification of the main types of degradations specific to the steam generator piping;<\/li><li>Identification of the causes and conditions of cracking corrosion under load on the steam generator piping;<\/li><li>Determination of the thickness layer of oxides and protective coatings on metal samples (beneficiary S.C.METIGLA SRL)<\/li><li>Corrosion rating of welded samples from duplex steels, according to ASTM G-48 (beneficiary SC DAMEN)<\/li><li>Recommendations for minimizing the effects of microbiological corrosion in raw water-cooled systems from Cernavoda NPP;<\/li><li>Identification of the corrosion behavior in liquid Pb medium, of 15Cr15Ti and 316L steels.<\/li><\/ul><p><strong><u>LADICON - CNCAN notified laboratory<\/u><\/strong><\/p><p class=\" translation-block\">The Laboratory for Analysis and Diagnosis of Corroded Metal Components in Nuclear Installations (LADICON) is part of the Nuclear Materials and Corrosion section and has as main objectives:<\/p><ul><li>analysis of degraded metal components using specific tests and characterization methods to identify the causes<\/li><li>identification of technical solutions to reduce \/ prevent the degradation phenomena,<\/li><li>evaluation of the corrosion behavior of metallic materials in different environments.<\/li><\/ul><p>The quality assurance of the tests within LADICON is performed in accordance with the requirements of the SR EN ISO \/ CEI 17025 standard, with the requirements of the clients and of the regulatory authorities in the field (CNCAN Bucharest). The laboratory is notified as a testing laboratory by CNCAN Notification no. LI-04_LADICON \/ 2020.<\/p><p><strong>Test \/ analysis methods<\/strong><\/p><ul><li>Determination of susceptibility to generalized and localized corrosion by gravimetric analysis and accelerated chemical tests;<\/li><li>Analysis by metallographic microscopy of metal components (measurement of oxide layer thickness \/ organic deposits \/ ceramic deposits, determination of average grain size, determination of non-metallic inclusions)<\/li><li>Determination of corrosion susceptibility of structural materials by electrochemical methods (variation of corrosion potential, linear polarization and cyclic polarization);<\/li><li>Identification of phase composition by X-ray diffraction (qualitative and quantitative analysis on polycrystalline materials, investigation of thin layers, determination of crystallite size and microtensions, quantitative analysis of internal stresses, X-ray diffraction at radiant incidence, microdiffraction).<strong>.<\/strong><\/li><\/ul><p><strong>Main achievements<\/strong><\/p><ul><li>Identification by X-ray diffraction analysis of the chemical composition and crystalline state of the corrosion products on the Milipore filters (beneficiary Cernavoda NPP)<\/li><li>Fault analysis of the rocker cover from a diesel engine from Unit 1 Cernavoda NPP \u00a0<\/li><li>Development of accelerated chemical methods: Determination of the minimum critical corrosion initiation temperature in the crevice for stainless steels; Determination of susceptibility to intergranular corrosion of welded joints\u00a0<\/li><li>Teste electrochimice de determinare a vitezelor de coroziune a materialelor metalice (beneficiar CNE\u00a0 Cernavod\u0103)<\/li><li>Analyzes by metallographic microscopy (beneficiaries Unit 1 Cernavoda NPP; SC METIGLA SRL)<\/li><li>Accelerated chemical tests to identify pitting corrosion (beneficiary Societatea \u0218antierul Naval DAMEN SA, Gala\u021bi)<\/li><\/ul><p><strong><u>Nuclear fuels<\/u><\/strong><\/p><p><strong>Activities<\/strong><\/p><ul><li class=\" translation-block\">Production of iridium disks, which will be used as irradiation targets in the TRIGA reactor and subsequently as closed radioactive sources of Ir192, used for industrial radiography.<\/li><li>Experimental research activities on the aging of concrete cladding structures.<\/li><li>Evaluation of the oxidation behavior of uranium dioxide fuel in severe accident conditions.<\/li><li>Experimental studies for the development of nitride fuels by the hydration-nitriding method.<\/li><li>Fuel-coolant interaction tests for LFR reactors.<\/li><li>Production of mixed thorium and uranium oxide powder by chemical method.<\/li><li>Production of mixed thorium and uranium oxide tablets.<\/li><li>Fabricarea de pastile\u00a0 de UO<sub>2<\/sub>\u00a0cu grad de \u00eembog\u0103\u021bire de 1\u00f710%\u00a0<sup>235<\/sup>U.<\/li><li>Fabricarea baghetelor combustibile pe baz\u0103 de uraniu slab \u00eembog\u0103\u021bit prin metoda \u00a0metalurgiei pulberilor.<\/li><li>Recuperarea uraniului sub form\u0103 de UO<sub>2<\/sub>\u00a0din produsele secundare rezultate la fabrica\u021bia baghetelor combustibile.<\/li><li>Construction of an installation for welding the ECE-LEU experimental fuel element.<\/li><li>Determination of optimal welding parameters by structural analysis and determination of mechanical properties.<\/li><li>Design and construction of an ECE-LEU vacuum chamber.<\/li><li>Studies and experimental research on the storage of hydrogen isotopes in the form of metal hydride.<\/li><\/ul><ul><li>Research on improving tritium management knowledge in the field of nuclear fission.<\/li><li>Participation in international projects in the field of tritium management in the field of nuclear fission and fusion (project H2020-TRANSAT).<\/li><\/ul><p><strong>Main achievements<\/strong><\/p><ul><li>Production of instrumented experimental fuel elements for irradiation in the TRIGA ICN reactor.<\/li><li>Production of iridium disks.<\/li><li>Obtaining U-Zr alloys with different content from Zr.<\/li><\/ul><p><strong><u>Analiza supreafe<\/u><\/strong><strong><u>\u021belor<\/u><\/strong><\/p><p><strong>Activities<\/strong><\/p><ul><li class=\" translation-block\">Surface treatment by electrolytic oxidation in plasma (PEO)<\/li><li>Analiza suprafe\u021bei prin spectroscopie de fotoelectroni cu raze X\u00a0<em>(Engl. XPS)<\/em><\/li><li>Characterization of corrosion resistance<\/li><\/ul><p><strong>Certifications<\/strong><\/p><ul><li>The laboratory is designated as a Notified Test Laboratory, according to the Notification LI 1_ESCALAB \/ 2020 issued by the National Commission for the Nuclear Activities Control (CNCAN).<\/li><\/ul><p><strong>Main achievements<\/strong><\/p><ul><li>Methods of obtaining ceramic coatings of mixed metal oxides resistant to corrosion and wear on Zr-2,5Nb and Titan alloys in order to increase their service life, presented in the last 5 years, in:<ul><li>33 research papers,<\/li><li>17 scientific articles indexed by ISI,<\/li><li>6 scientific articles indexed in international databases,<\/li><li>7 scientific papers presented at conferences (national and international).<\/li><\/ul><\/li><\/ul><ul><li>Training students in their final years in the field of obtaining ceramic coatings by the technique of plasma electrolytic oxidation (PEO) and their characterization by the technique of X-ray electron spectroscopy (XPS) by supporting, in the last 5 years,:<ul><li>6 bachelor's \/ dissertation papers.<\/li><\/ul><\/li><\/ul><p><strong>\u00a0<\/strong><\/p><p><strong>Contact person<\/strong> CS III Alexandru-Ionut Nitu, e-mail: <a href=\"mailto:alexandru.nitu@nuclear.ro\">alexandru.nitu@nuclear.ro<\/a><\/p>\t\t\t\t\t\t<\/div>\n\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>\n\t\t<\/div>\n\t\t\t\t\t\t\t<\/div>\n\t\t<\/section>\n\t\t\t\t\t\t<\/div>\n\t\t\t\t\t<\/div>","protected":false},"excerpt":{"rendered":"<p>Propriet\u0103\u021bi Termomecanice \u0219i Analize Microstructurale Activit\u0103\u021bi Analiza microstructural\u0103 prin tehnici de microscopie optic\u0103, electronic\u0103 de baleiaj (SEM) \u0219i spectrometrie de raze X cu dispersie dup\u0103 energie, a materialelor metalice \u0219i ceramice; Teste termo-mecanice pe materiale metalice,\u00a0 ceramice \u0219i compozite \u00een intervalul de temperatur\u0103 20 \u00f7 1000oC (trac\u021biune, fluaj, ciclaj, mecanica ruperii); Teste de explozie pe&hellip;<\/p>","protected":false},"author":1,"featured_media":0,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":[],"categories":[4],"tags":[],"yoast_head":"<!-- This site is optimized with the Yoast SEO plugin v17.6 - 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